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kilomentor

Checklist for Developing a Scaled up Step in a Chemical Process

kilomentor | 30 December, 2006 18:55

  1. This site will be presenting strategies for efficiently creating rugged chemical processes. By processes we mean a series of chemical steps and isolations which produce commercially interesting amounts of pure substances- my own experience of 40 years is with pharmaceutical actives. Here we get started by just considering some of the questions which a process chemist asks hinself/herself about a proposed transformation.
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Comparison of Preparative Chromatography Methods

kilomentor | 30 December, 2006 15:01

In organic chemistry, product isolation and purification is the most time consuming aspect of the art. It is the least intensively dealt with in the literature. Because preparative column chromatography is by far the most general and powerful of these methods, a thorough understanding of the available options is important. Over the years some highly refined and powerful methods have been designed for carrying out preparative scale separations; however, there has been no comprehensive description, tabulation or critical comparison of these second and third generation forms of preparative chromatography. This is the goal.

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