kilomentor

The Use of the Diisopropyl ether (DIPE) Water Azeotrope as a possible means to dry high boiling dipolar aprotic solvents

kilomentor | 28 December, 2009 19:17

The Kilomentor Blog is now being continued and updated at www.kilomentor.com this particular article appears at http://www.kilomentor.com/2009/12/the-use-of-the-diisopropyl-ether-dipe-water-azeotrope-as-a-possible-means-to-dry-high-boiling-dipolar-aprotic-solvents

 (More)

Nitriles Separated by Competitive Reaction and then Simple Extraction

kilomentor | 15 December, 2009 18:55

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article ca be found at http://www.kilomentor.com/2009/12/nitriles-separated-by-competitive-reaction-and-then-simple-extraction

 

Crystallization of miconized pharmaceuticals from impinging stream technology will soon be free to use.

kilomentor | 12 December, 2009 15:06

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/12/crystallization-of-miconized-pharmaceuticals-from-impinging-stream-technology-will-soon-be-free-to-use

 

The Possibility of Using Solid Alumina or Silica Gel Catalysis in Development of an Organic Synthetic Step

kilomentor | 26 November, 2009 19:04

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/11/the-possibility-of-using-solid-alumina-or-silica-gel-catalysis-in-development-of-an-organic-synthetic-step

   (More)

Recent Assessments of Organic Synthesis as expressed in Chemical Process Development

kilomentor | 25 October, 2009 17:32

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/10/recent-assessments-of-organic-synthesis-as-expressed-in-chemical-process-development

 

Selective Ester Hydrolysis as a Process Isolation Tool for Work At Scale

kilomentor | 09 October, 2009 03:52

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/10/selective-ester-hydrolysis-as-a-process-isolation-tool-for-work-at-scale

 

 

Explaining Process Intensification to Process Chemists

kilomentor | 03 October, 2009 17:14

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/10/explaining-process-intensification-to-process-chemists

Purification by Reaction: An Example of Removing a Serious Impurity by Purifying Starting Material

kilomentor | 27 August, 2009 17:23

 The Kilomentor Blog is now being continued and updated at www.kilomentor.com this particular article is available at http://www.kilomentor.com/2009/08/purification-by-reaction-an-example-of-removing-a-serious-impurity-by-purifying-starting-material

 

 

The Yoshida Tag Methodology and the Kilomentor Synthesis Philosophy

kilomentor | 16 August, 2009 05:08

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article is available at http://www.kilomentor.com/2009/08/the-yoshida-tag-methodology-and-the-kilomentor-synthesis-philosophy

 (More)

Understanding Distillation is still important for Chemical Process Development and Organic Synthesis At Scale.

kilomentor | 25 June, 2009 15:12

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article is available at http://www.kilomentor.com/2009/06/understanding-distillation-is-still-important-for-chemical-process-development-and-organic-synthesis-at-scale

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Chemical and Pharmaceutical Process Development Update Materials from the Earlier Kilomentor Articles (September 2007-September 2008)

kilomentor | 25 June, 2009 14:57

IThe Kilomentor Blog is now being continued and updated at www.kilomentor.com

 have seen a large increase in traffic to this blog after I reviewed the titles of some articles from April 2007 to September 2007. Therefore, I continue with this updating.

Search engines have the shortcoming that they give higher rankings to recent material. This is appropriate for news, fashion and opinion but not nearly as appropriate for scientific educational materials. Thus with the passage of time it becomes harder to locate pertinent kilomentor blogs. To counteract this I am providing a review of the titles of some of the early Kilomentor articles. Regular readers can of course find all my articles in the Kilomentor archives in the kilomentor blog.

 

The Use of Mesityl Oxide as a Dehydrating Agent by the Chemical Reaction of Water catalyzed by Primary Amines

Extraction and Phase Switching Hydrolysis-Purifying Phenols.

Avoiding the Impurity from Hell:(chemical process development; purification of organic chemicals; process optimization; impurity identification in organic synthesis)

Reactions “On Water” (immiscible water makes a great heat sink)

Kilomentor moves the discussion from Steam Distillation to other Co-distillations

Polymorphism in Organic Syntheses, Process Development and Formulation

Inverted Filtration: A chemical synthesis laboratory technique particularly helpful at 5-10 litre scales.

Recovering More Product by Crystallization in Organic Synthesis:Trituration with a modified water phase as a potential Chemical Process Development Method

The Complete Blog for the Preparation of Pharmaceutical Salts

Kilomentor weighs in as “Pharmaceutical Manufacturing Goes Green”.

Another Way to Separate Phenolics by Crystallizing of Co-crystals?

Green /Recyclable Solvents: Low Vapour pressure compositions for storage and recycling of solvents that are highly volatile or gaseous at room temperature

Symmetrical Bis-N,N-(3-nitrophenyl)urea: A Super Co-crystal Former that might have applications in Product Purification.

The Importance of the Molecular Weight of a Salt Former in choosing a Pharmaceutical Salt (the choice of salt is not as broad as you think)

Pamoates or Embonates: crystalline Pharmaceutical Salts or Derivatives for Isolation and Purification

Biocatalytic Methods of Enantioselective Synthesis in Pharmaceutical Process Development

Separation by Substantial Differences in Chemical Reactivity of the Same Nominal Functional Group.

Sulfate Pharmaceutical Salts

Kilomentor suggests some crazy purification ideas

kilomentor | 03 June, 2009 19:47

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article is available at http://www.kilomentor.com/2009/06/kilomentor-suggests-some-crazy-purification-ideas

 

Recycling Mother Liquors in Chemical Process Development to Raise Yields and Reduce Solvent Usage

kilomentor | 18 May, 2009 09:26

 The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article is available at http://www.kilomentor.com/2009/05/recycling-mother-liquors-in-chemical-process-development-to-raise-yields-and-reduce-solvent-usage

 

A Potential Widely Applicable Solution for Resolving Chiral Bases

kilomentor | 28 April, 2009 14:41

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/04/a-potential-widely-applicable-solution-for-resolving-chiral-bases

 

Extractive and Phase Switching Hydrolysis in Chemical Process Development.

kilomentor | 14 March, 2009 12:26

The Kilomentor Blog is now being continued and updated at www.kilomentor.com This particular article appears at http://www.kilomentor.com/2009/03/extractive-and-phase-switching-hydrolysis-in-chemical-process-development

 

 

 

 

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